Master the intricacies of X-ray diffraction (XRD) with this definitive guide. Dive deep into essential procedures for analysing polycrystalline and amorphous materials. This comprehensive text explains fundamental theory, practical techniques, sample preparation, and data interpretation, crucial for uncovering material structures and properties. An indispensable resource for students, researchers, and scientists in physics, chemistry, materials science, and mineralogy across India seeking to excel in analytical techniques.