Master essential microscale organic laboratory techniques with this comprehensive practical guide. Designed for Indian university curricula, it offers hands-on experience with modern microscale methods for synthesis, purification, and characterization. Explore spectroscopy (IR, NMR, UV-Vis, MS) and qualitative analysis, vital for identifying organic compounds. An indispensable resource for B.Sc. and M.Sc. Chemistry students, researchers, and educators nationwide, ensuring proficiency in experimental organic chemistry.